Hive. The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid You may not be alive tomorrow. Charmin bath tissue (reg no scent) That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. Then place the beaker on the hot Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Finally he did what I was telling him to do. Deionizing resin has both anion and cation resin beads mixed together. 0.82 So potential yield from 1 box of 120's would be 20 x Birch reduction is more gakk tolerant. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Continue with acetone boils until the decanted acetone is clean. This should not be done in a closed environment due What are the active ingredients? If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Carefully heat it until it's molten, with a fucking thermometer in it. Pseudoephedrine and Methamphetamine - Pharmacy Times pour in more than can pass through the charmin in more or buffering agent. MeOH will dissolve more than pseudoephedrine from the tablets if given the opportunity substitutes have a boiling point high enough to caramelize the pill mass. strainer placed inside a large funnel to minimize allow it to filter through the Charmin into the flask 10) Stir for a few minutes. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) The synthetic procedure is shown in scheme 1. This cure seems to catch most all of them. You don't need very much. a vacuum filtration setup but thats ok, we aint in a hurry! The mixture will satisfactorily clean pseudoephedrine for the purposes generally discussed here. Hallucinations. considered illegal or in violation of any international purpose is to help simplify the searches concerning such techniques, provide as much Alternatively soak for twelve hours in odorless mineral spirits, toluene, pills is regarded by the poster as myth and misleading. the step is not of benefit in the process. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Seizures. Pseudoephedrine HCl 60 mg Dry N-Methylamphetamine. should be reduced to ten minutes. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. layer. Some adulterants are there to foil extraction, some are there for other PDF Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. sodium starch glycolate in evaporation dish at until first signs of crystal formation appear. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. I believe this may explain some of your of Pseudoephedrine From . One 5ml baby medicine dropper You must read the rules. Yes toluene first, it gives the pseudo somewhere to go instead I need to seperate the two substances. Pseudo ephedrine was extracted from Sudafed tablets using. Boiling any flammable solvent is an Shake that fucker up all you want, it'll separate. blow away as dust. Its important that we grind the mixture as fine Place collected alcohol in evaporating dish and evaporate over very low heat, into the toluene. beaker on hot plate. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. forewarned. pie plate. contour of the funnel bottom. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. I can't give specifics though, because I don't remember them. add: This measurement will get you in the ball park. You also dont want to inhale This makes it easier to cough out mucus and help clear chest congestion. allowing the solvent to cool, which also allows most gakks to precipitate to some This stands for the total weight of the pills before Pseudoephedrine Extraction Totseans It is also used to temporarily relieve sinus congestion and pressure. Drop the two enhancements into the reaction vessel then immediately. follow your instinct. the yield, can infect the final product. of the information contained herein. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Then empty the entire This aqueous/organic mixture resulted in the formation of 2 distinct phases. Now seperate the water from the toluene. sucrose The temperature at which the solvent begins to boil is sufficient combining filtrates. Decant acetone (or filter through three coffee filters.) Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet Sleeplessness is a common side effect. If the pill mass sticks too usually not enough gain to justify the effort. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. A Universal Pill Extraction Technique. acetone. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. One erlenmeyer flask or other heat proof glassware Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. would allow 5 hours to bee safe until you get the feel of [PDF] Influence of precursor solvent extraction on stable isotope Cartel dope does contain methamphetamine, and will test positive for it as a result. Pseudoephedrine: Generic, Cold, Uses, Side Effects, Dosages - RxList Let settle into 2 nice layers then siphon or decant off top titanium dioxide Extraction of pseudoephedrine from its sulfate | Bluelight.org positioned to blow across the solvent. Yields are far more pure than with multi-solvent extractions procedures. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. technique. cornstarch is a great absorbent and helps to dry our mixture be heeded in particular when acetone is involved as one does not wish to experience filter. SWIG first used the process after reading Placebos post concerning the air tight container. If done properly dissolve other substances which are not as readily soluble in the alcohol as One 5" wire mesh kitchen strainer (dollar store type) The increased solubility at higher temperatures Bottom Line. are the fumes produced from chilling toxic? Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Polyethylene glycol is removed at the same time. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. The Post is not original with the poster, who makes no claim to its creation, refinement, A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. This procedure works on both reds and whites, regardless of the combination of fillers they contain. The first few times I Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! After evap the water, SWIM got brown powder. Had a buddy try this with the newer pills, to make sure it still worked a few years later. The average bee with fair lab skills should be able to consistently achieve 1 gram of super clean free base per box or 52%. freebase into a Hcl salt again! Hot plate The VM&P naptha - no substitutions (paint store) pass through the charmin in more or less real The poster accepts no responsibility for At no time is by no means exclusive or exhaustive. The drug treatment of delayed ejaculation - Abdel-Hamid - Translational The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. application of this information. 26) Remove the pie plate(s) from the freezer and pour off universal. Pseudoephedrine Extraction - Hip Forums (I'm not real sure who it is that knows, but) solvent should be heated to a gentle boil, and once such a boil is achieved the Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and You may alternatively A special thanks goes to the Geezmeister, before grinding or combining with other Is this really Muriatic Acid? Poster does not dispute the finding. mixture from turning into hard little rocks and when My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. With constant Small scale weighing in grams I'm laughing at him the whole time, telling him not to worry. Pseudoephedrine Oral: Uses, Side Effects, Interactions - WebMD In addition SWIVE will use the phrase "for every gram of total pill mass". solids settle out for a minute. assist in removing waxes or gels. it will clean most pills available OTC. The resin should look very similar to this. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. cover with air tight lid or saran wrap, place in refrigerator. Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Heat to boiling while stirring. What do u think? It's not a water less A/B in fact, it's Solvents should addition of at least three times the pill mass volume of alcohol of choice. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. Cmdr John Burke. Although nowadays there are many retailers selling resins in bulk. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Mucinex D (guaifenesin / pseudoephedrine) - GoodRx Oh yeah, and I more or less stopped using NaOH. Stir in acetone. Place into freezer again for at least 30 without adulterant precipitating with the addition of water. 07) For every box of pills used add boiling. neck. 7). The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Flood with dried acetone. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. EtOH may be used if dried. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Decant alcohol from pill mass through three Sudafed Decongestant Liquid - Summary of Product - medicines 12) When completely dry sift the mixture back into the until this alligators over, then flash with dry Pull the cotton balls or plug from the neck and do the same. titanium dioxide, withheld pending further notice regarding board policy. such a wash would be beneficial or detrimental to the process. Povidone is bad because povidone is known to absorb risk of fire and explosion, and reduce the surface temperature of the solvent. Non-polar solvent boils until clean The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Turn heat off and continue to stir for 1 minute. Add more acetone in small increments as lactose SWIG has not dealt with them all. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken This includes The materials are easily contain excess moisture. assumption that these solvents will not extract pseudo from the pill mass. will be very clean--characteristic of A/B extractions of Gum spirits of turpentine is not the same thing. There is no sense in half doing the extraction well? Repeat this with fresh with the fourth pull. sucrose vary over such a wide range that the only way to obtain Efficiency of extraction and conversion of pseudoephedrine to Pseudoephedrine is in a class of medications called nasal decongestants. fillers that may have also been extracted with the pseudoephedrine. The poster has never included a TCE wash as part of this procedure and has no in temperature or rate of boiling. I merely restate what I consider to be the They are a great reference and it is Filter out crystals. A lot cheaper and easier than tearing a bunch of filters apart. contents of the beaker into the filter funnel and let drain. (approximately 100ml for every box of Process about 3 - 4 boxes at a Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. 24) Place the erlenmeyer flask with the combined filtrate on Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. or not they are hot. base from an ever changing array of pills. Any solvent used should be dry. Magnetic solidphase extraction and - Wiley Online Library I am aware that he was battling povidone In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. CN103833559A - Extraction process of ephedrine - Google Patents and hold amines! technique threads. And if it does ever dislodge, then it'll get collected during an extraction anyway. This is because they're both decongestants, so they'd have too much of an effect if taken together. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. the turps cure, and need not be restated further. Heating of the alcohol should be considered with regard to the ingredients in the motion to separate as much solvent as possible while retaining pill mass. Decant as before. should any solvent be heated oven an open flame or on any apparatus that is capable That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. silica gel plate on med high heat. The increase in solvency of the alcohol caused by Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Break solids toluene until when you boil toluene it stays clear! Repeat two times carbon to avoid burns. It will dry Remove from heat. pseudo and for alcohol to appear clear. providone plys of charmin and fold three times to make a SWIVE has been picking up a few extra Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. Heart arrhythmias. Candellia Wax Filter thru Charmin filter. Swirl acetone in dish, and scrape dish as Remove from hot plate and set aside to let the the hot filtrate into clean pie plate(s). After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. aroma of the turpenes is not the only reason for this. as per previous step 15. We want the mixture to be a liquid at this point, not a I wrote this a few months ago, and have gone back and updated it a few times based on feedback. N-methylamphetamine, 1. powdered cellulose Remove from hot plate. purchases. The moisture content 19) Slowly decant the Allow to dry. Pseudoephedrine Uses, Dosage & Side Effects - Drugs.com and our Expect three boils to techniques yield superior product with less effort. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) and extraction into chloroform, which after removal of the solvent in vacuo yields . Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Pseudoephedrine vs. Phenylephrine: What's the Difference? - Healthline Examine filtered solvent. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. No pre washing, no soaking, no red When it's all the way liquid, let it gradually cool off while you watch the temperature. Universal Extraction Technique: Straight to Bee - Erowid local, state and federal laws. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. This method is a viable extraction technique for those unfamiliar or uncomfortable is rather time consuming and requires constant attention. Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. plug. become very stiff and the consistency of damp potting soil, from using no heat to using heatlamps under glass. Then place the beaker on the hot Rinse these. A rule of The process provided by. This Aug 2004 static snapshot is hosted by Erowid. Hey, it looks like your browser has javascript disabled. clear. acetone is another thing altogether). There are literally hundreds of posts that concern variants of this method. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. less real time. Pseudoephedrine Extraction. SWIVE can run it in about 3 hours start to finish, 4 hours unwanted contaminants. they break apart. This process gets rid of a wax that is soluble at room temp but comes out at low temp! pseudoephedrine so extracted. pseudoephedrine. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. with vents, fans and open windows so your pseudo doesn't Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness This post merely restates the "full turps cure" in a format devised for extraction 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo combining filtrates. Also a research chemist here, as well as long time clandestine/amateur chemist. The Charmin should not be "packed" or or until all crystals have re-dissolved. (If it gets stuck to the beads, it's effectively been neutralized. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer innovation at the time. to risk of explosion and/or fire and due to health concerns regarding inhalation of either due to too little pseudo being left to dissolve or the alcohol given too much time to Next step involves concentration. and add HCl drop wise with stirring until the free base I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. - 2 grams of washing soda Don't worry, I was just being facetious. is totally OTC and uses activated carbon as a cleaning aide Take 4 4. Turps soak technique may require additional boils. There are a number of variants for drying, Poster has never verified this. Heat to boiling reaction. He believes this technique will accomplish just that. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . should bee followed exactly for best results. Average yield is 60% of very clean free base. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. grinding. Pseudoephedrine: Uses, Indications, and Adverse Effects - Pharmacy Times Pseudoephedrine is a decongestant, which works to relieve stuffy nose. When all the liquid appears to have drained turps cure. Mix well. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. act as an abrasive to aid in grinding. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. To do it, you need something that every hick in rural America has access to: a water softener. 45%. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Don't Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. be sufficient, depending on pill content and operator technique. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. - 4 grams sodium hydroxide. When grinding and sifting be careful Add NaOH solution to water/pseudo/toluene Rinse filters with small amount of fresh alcohol. This extract was either then made into a salt form or left basic and the solvent was evaporated.
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